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Mass Spectral Characterization of Naphthoquinones Related to Lapachol

✍ Scribed by Girard, M.; Ethier, J.-C.; Kindack, D.; Dawson, B. A.; Awang, D. V. C.

Book ID
127324047
Publisher
American Chemical Society
Year
1987
Tongue
English
Weight
196 KB
Volume
50
Category
Article
ISSN
0163-3864

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A preparative synthesis of lapachol and
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The lithium salt of 2-hydroxy-l,4-naphthoquinone was prepared in situ by addition of lithium hydride to the frozen solution of the quinone in dimethyl sulfoxide. As the solution thawed, the lithium quinone was slowly formed and was then alkylated with 3,3-dimethylallyl bromide. Lapachol was thus obt

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