MAS NMR structure refinement of uniformly 13C enriched chlorophyll a/water aggregates with 2D dipolar correlation spectroscopy

A 3-D Structural Model of Solid Self-Ass

A 3-D Structural Model of Solid Self-Assembled Chlorophyll a/H2O from Multispin Labeling and MAS NMR 2-D Dipolar Correlation Spectroscopy in High Magnetic Field

✍ Barth J. van Rossum; Els A.M. Schulten; Jan Raap; Hartmut Oschkinat; Huub J.M. d 📂 Article 📅 2002 🏛 Elsevier Science 🌐 English ⚖ 607 KB

## Magic angle spinning (MAS) NMR with Lee-Goldburg crosspolarization (LG-CP) is used to promote long-range heteronuclear transfer of magnetization and to constrain a structural model for uniformly labeled chlorophyll a/H 2 O. An effective maximum transfer range d max can be determined experimenta