✦ LIBER ✦
Mapping out the connectivities in intermediate gel phases of molecular sieve synthesis by solid-state NMR
✍ Scribed by Yining Huang; David Machado
- Publisher
- Elsevier Science
- Year
- 2001
- Tongue
- English
- Weight
- 143 KB
- Volume
- 47
- Category
- Article
- ISSN
- 1387-1811
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✦ Synopsis
The present communication demonstrates, for the ®rst time, that 31 P/ 27 Al double resonance solid-state NMR experiments such as cross-polarization (CP) can be used to map out the connectivity in the intermediate gel phases of molecular sieve synthesis. Our work clearly highlights the advantages of using Al/P CP techniques for characterizing the gel phases.