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Main group metal(II) tetrafluoroborate interactions with 2,6-lutidine N-oxide

✍ Scribed by Chester M. Mikulski; Larry S. Gelfand; Ellen S.C. Schwartz; Louis L. Pytlewski; Nicholas M. Karayannis


Book ID
115976747
Publisher
Elsevier Science
Year
1981
Weight
265 KB
Volume
43
Category
Article
ISSN
0022-1902

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The reaction of PhN 3 (H)C 6 H 4 N 3 (H)Ph with Hg(NO 3 ) 2 in THF in the presence of triethylamine yields {Hg[PhN 3 C 6 H 4 N 3 (H)Ph](NO 3 )} as a yellow powder that can be recrystallized from THF/acetone. The crystals belong to the monoclinic system, space group P2 1 with the cell dimensions a Ο­