The design of a solenoidal NMR coil with high-B 1 homogeneity turns and thus to significant field variations in the vicinity for high-frequency solid-state NMR is described. The coil is made of the conductor. This effect is particularly pronounced at of thin ribbon of continuously variable width. Th
Magnet Design with High B0 Homogeneity for Fast-Field-Cycling NMR Applications
β Scribed by O. Lips; A.F. Privalov; S.V. Dvinskikh; F. Fujara
- Publisher
- Elsevier Science
- Year
- 2001
- Tongue
- English
- Weight
- 295 KB
- Volume
- 149
- Category
- Article
- ISSN
- 1090-7807
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β¦ Synopsis
The design, construction, and performance of a low-inductance solenoidal coil with high B 0 homogeneity for fast-field-cycling NMR is presented. It consists of six concentric layers. The conductor width is varied to minimize the B 0 inhomogeneity in the volume of the sample. This is done using an algorithm which takes the real shape of the conductor directly into account. The calculated coil geometry can be manufactured easily using standard computerized numeric control equipment, which keeps the costs low. The coil is liquid cooled and produces a B 0 field of 0.95 T at 800 A . The field inhomogeneity in a cylindrical volume (diameter 5 mm, length 10 mm) is about 10 ppm, and the inductance is 190 Β΅H. Switching times below 200 Β΅s can be achieved. During 6 months of operation the coil has shown good stability and reliability.
π SIMILAR VOLUMES
Since the classical treatment by Torrey in 1949 of the problem of how magnetization evolves in a continuously applied B radiofrequency field, the topic has 1 received relatively little attention in the nuclear magnetic resonance literature. This article focuses on the behavior of the macroscopic mag