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Macromolecular NMR spectroscopy for the non-spectroscopist

✍ Scribed by Ann H. Kwan; Mehdi Mobli; Paul R. Gooley; Glenn F. King; Joel P. Mackay


Book ID
111313822
Publisher
John Wiley and Sons
Year
2011
Tongue
English
Weight
786 KB
Volume
278
Category
Article
ISSN
1432-1327

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A tritium labelled phospholipase A2 (PLA2) amide analogue inhibitor was prepared by the reduction of an alkene precursor. Diimide, heterogeneous and homogeneous metal catalyzed reduction methods were assessed for their suitability for the preparation of a tritiated ligand for 3H NMR spectroscopic st