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Low temperature1H NMR study of electronic structure parameters (T1eT) in zirconium dihydride

✍ Scribed by O. J. Żogal; A. H. Vuorimäki; E. E. Ylinen; K. Niedźwiedź

Book ID
112514485
Publisher
Springer
Year
1995
Tongue
English
Weight
285 KB
Volume
96
Category
Article
ISSN
1434-6036

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✍ G. W. Buchanan; M. Gerzain; K. Bourque 📂 Article 📅 1997 🏛 John Wiley and Sons 🌐 English ⚖ 434 KB 👁 2 views

Two conformations of cis-cyclohexyl-10-crown-3 were detected in solution below 250 K using 1H NMR at 400 MHz and 13C NMR at 100 MHz. Chemical shift assignments were facilitated by spectra of two dideuterio derivatives. From relative peak area measurements, the conformation with the unit OÈCH 2 ÈCH 2