Low-temperature thermodynamics of Ln(Me2dtc)3(C12H8N2) (Me2dtc
✍ Scribed by Jian Wu; San-Ping Chen; You-Ying Di; Sheng-Li Gao
- Book ID
- 106446884
- Publisher
- Springer Netherlands
- Year
- 2009
- Tongue
- English
- Weight
- 432 KB
- Volume
- 100
- Category
- Article
- ISSN
- 0022-5215
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Reaction of the diamidopyridine protio-ligand MeC(2-C 5 H 4 N){CH 2 N(H)Mes} 2 (Mes = 2,4,6-C 6 H 2 Me 3 ) with butyllithium in diethyl ether affords the compound (diethyl ether)( 4 -2-{6- [1,4,6 shows the methylation of the pyridyl ortho-position with a methyl group of one of the mesityl groups. T
lo6 pm3, Messung bei -80°C. ebDr = 2.16 p = 92.7 em-', Z = 4, orthorhombisch, Pnrna (Nr. 62), Enraf-Nonius CAD-4. 1 . =71.07 pm (Mo,,. Graphit-Monochromator), w-Scan, 3002 gemessene Reflexe (+ h, + k, k I), davon 1211 unabhangig, 1104 mit I > 3u(I) zur \'erfeineruiig benutzt, Strukturlosung mit Patt