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Low-Temperature Preparation of La0.6Sr0.4Fe0.8Co0.2O3–δ Sinterable Nanopowders by the Polymeric Organic Complex Solution Method

✍ Scribed by J. M. Perez-Falcon; A. Moure; J. Tartaj


Publisher
John Wiley and Sons
Year
2010
Tongue
English
Weight
789 KB
Volume
11
Category
Article
ISSN
1615-6846

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✦ Synopsis


Abstract

In this work, powders of La~0.6~Sr~0.4~Fe~0.8~Co~0.2~O~3–δ~ were prepared by the auto‐combustion of ethylene glycol–metal nitrate polymerised gel precursor. This method (polymeric organic complex solution) allows decreasing the processing temperature and simplifies the whole procedure. A single phase material is obtained at 300 °C lower than that needed by conventional solid state reaction (SSR). The reduced particle size and low agglomeration increases the reactivity of powders and therefore, the sintering temperature is also reduced in 200 °C with respect to the conventional SSR method. As a consequence of that, the microstructures are controlled maintaining the grain size in an almost nanometric range.


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