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Low-Molecular-Weight Poly(α-methyl β,L-malate) of Microbial Origin: Synthesis and Crystallization

✍ Scribed by Carlos E. Fernández; Manuel Mancera; Eggehard Holler; Jordi J. Bou; Juan A. Galbis; Sebastián Muñoz-Guerra


Publisher
John Wiley and Sons
Year
2005
Tongue
English
Weight
212 KB
Volume
5
Category
Article
ISSN
1616-5187

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✦ Synopsis


Abstract

Summary: Low‐molecular‐weight poly(α‐methyl β,L‐malate) made of approximately 25–30 units was prepared from microbial poly(β,L‐malic acid) by treatment with diazomethane. The thermal characterization of the polymalate methyl ester was carried out and its crystalline structure was preliminary examined. Its ability to crystallize both from solution and from the melt was comparatively evaluated.

Poly(α‐methyl β,L‐malate) spherulitic film cast from CHCl~3~.

magnified imagePoly(α‐methyl β,L‐malate) spherulitic film cast from CHCl~3~.