𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Long-Range Correlations between Aliphatic 13C Nuclei in Protein MAS NMR Spectroscopy

✍ Scribed by Marvin J. Bayro; Thorsten Maly; Neil R. Birkett; Christopher M. Dobson; Robert G. Griffin


Publisher
John Wiley and Sons
Year
2009
Tongue
English
Weight
343 KB
Volume
121
Category
Article
ISSN
0044-8249

No coin nor oath required. For personal study only.


📜 SIMILAR VOLUMES


2D13C–13C MAS NMR Correlation Spectrosco
✍ Ido de Boer; Leon Bosman; Jan Raap; Hartmut Oschkinat; Huub J.M. de Groot 📂 Article 📅 2002 🏛 Elsevier Science 🌐 English ⚖ 129 KB

An improved 2D (13)C-(13)C CP(3) MAS NMR correlation experiment with mixing by true (1)H spin diffusion is presented. With CP(3), correlations can be detected over a much longer range than with direct (1)H-(13)C or (13)C-(13)C dipolar recoupling. The experiment employs a (1)H spin diffusion mixing p

Quantitative Correlation between Steric
✍ Luigi Abbondanza; Luigi Abis; Nicoletta Cardi; Fabio Garbassi; Riccardo Po 📂 Article 📅 2003 🏛 John Wiley and Sons 🌐 English ⚖ 180 KB

## Abstract Several syndiotactic polystyrene (sPS) samples have been synthesized by using different catalytic systems. Their stereochemistry has been determined by ^13^C NMR spectra in both the aliphatic CH~2~ and aromatic C~1~ resonance regions. The observed peaks have been unambiguously assigned

Long-range 19F15N distance measurements
✍ Daniel T. Graesser; Benjamin J. Wylie; Andrew J. Nieuwkoop; W. Trent Franks; Cha 📂 Article 📅 2007 🏛 John Wiley and Sons 🌐 English ⚖ 469 KB

We present a novel rotational-echo double resonance (REDOR) method for detection of multiple 19 F-15 N distances in solid proteins. The method is applicable to protein samples containing a single 19 F label, in addition to high levels of 13 C and 15 N enrichment. REDOR dephasing pulses are applied o