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Linear analysis of carbon-13 chemical shift differences and its application to the detection and correction of errors in referencing and spin system identifications

✍ Scribed by Liya Wang; Hamid R. Eghbalnia; Arash Bahrami; John L. Markley

Publisher
Springer Netherlands
Year
2005
Tongue
English
Weight
457 KB
Volume
32
Category
Article
ISSN
0925-2738

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13C NMR spectra of para-substituted methoxybenzenes and phenols were recorded in the solid state to gain an insight into the manner and origin of substantial peak splittings in the ortho (up to 9.2 ppm) and mefa (up to 2.5 ppm) carbon signals. It was difficult to account for these peak splittings on