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Lead tetraacetate oxidation of the oxime of pregna-5,16-dien-3B-acetoxy-20-one

✍ Scribed by Kaufmann, Stephen; Tokes, L.; Murphy, J. W.; Crabbe, P.

Book ID
126202451
Publisher
American Chemical Society
Year
1969
Tongue
English
Weight
531 KB
Volume
34
Category
Article
ISSN
0022-3263

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Synthesis and oxidation of pregna-3,5-di
Synthesis and oxidation of pregna-3,5-dien-20-ols and -20-one and selective reduction of pregna-3,5-dien-20-one
✍ Göndös, György ;Orr, James C. 📂 Article 📅 1990 🏛 John Wiley and Sons 🌐 English ⚖ 248 KB

## Abstract Pregna‐3,5‐dien‐20‐one (4) and (20S)‐ and (20R)‐pregna‐3,5‐dien‐20‐ol (2 and 3) were synthesized from progesterone. Oxidation of a mixture of 2 and 3 with Jones reagent gave 4, while a large excess of Jones reagent afforded besides 4, 6‐oxoprogesterone (5), 6β‐hydroxyprogesterone (6) an