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Lead indium bismuth chalcogenides. III. Structure of Pb4In2Bi4S13

✍ Scribed by Krämer, V.

Book ID
114503609
Publisher
International Union of Crystallography
Year
1986
Tongue
English
Weight
298 KB
Volume
42
Category
Article
ISSN
0108-2701

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✍ Sophie Giraud; Jean-Pierre Wignacourt; Michel Drache; Guy Nowogrocki; Hugo Stein 📂 Article 📅 1999 🏛 Elsevier Science 🌐 English ⚖ 300 KB

Pb 4 BiO 4 PO 4 was prepared by heating a stoichiometric mixture of (NH 4 ) 2 HPO 4 , PbO, and Bi 2 O 3 at 700°C for 4 days with intermediate grinding. The material melts congruently at 805°C; single crystals were obtained by slow cooling of a melt. The compound is triclinic, P1 , a ‫؍‬ 6.215(1) A s