## Background: Large amounts of na,k-atpase are needed for studies involving protein chemistry. preparation of na,k-atpase from kidney by the widely used, rapid procedure of jΓΈrgensen (biochim biophys acta 356:36-52, 1974; methods enzymol 156:29-43, 1988) includes labor-intensive dissection of tiss
β¦ LIBER β¦
Large-scale preparation of perchlorates directly from sodium chloride
β Scribed by H. V. K. Udupa; K. C. Narasimham; M. Nagalingam; N. Thiagarajan; G. Subramanian; R. Palanisamy; S. Pushpavanam; M. Sadagopalan; V. Gopalakrishnan
- Publisher
- Springer
- Year
- 1971
- Tongue
- English
- Weight
- 407 KB
- Volume
- 1
- Category
- Article
- ISSN
- 0021-891X
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The synthesis of a variety of enantiomerically pure chiral auxiliaries based on (S)-proline and bearing sterically demanding side chains at the pyrrolidine moiety, such as the secondary amines (s)-2,5 and 2 and the hydrazines (S)-a, is described on a molar scale. As key step, the Grignard or RLi add