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Large scale isolation of 1,2:3,4-di-O-isopropylidene-α-d-glucoseptanose and 2,3:4,5-di-O-isopropylidene-β-d-glucoseptanose

✍ Scribed by John D. Stevens

Book ID
108080788
Publisher
Elsevier Science
Year
2011
Tongue
English
Weight
165 KB
Volume
346
Category
Article
ISSN
0008-6215

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X-ray and conformational investigation o
X-ray and conformational investigation of 6-deoxy-6-C-(1,5-di-O-acetyl-2,3-O-isopropylidene-β-d-allo-pentofuranos-5-yl)-1,2:3,4-di-O-isopropylidene- α-d-galactopyranose and 6-C-(benzyl 5-deoxy-2,3-O-isopropylidene-β-d-ribofuranosid-5-yl)-1,2:3,4-di-O-isopropylidene- d-glycero-α-d-galacto-hexopyranose
✍ Janusz W. Krajewski; Wojciech Karpiesiuk; Anna Banaszek 📂 Article 📅 1994 🏛 Elsevier Science 🌐 English ⚖ 523 KB

The structures of the title compounds (2b and 3) have been investigated in the solid state by X-ray methods. The crystals of 2b are monoclinic, space group P2,, and of 3 orthorhombit, space grtup P2,2,2,. The cell dimensions are: for 2b, a = 9.910(2), b = 11;745W, c = 11.810(3) A, /3 = 97.32(l)"; a