โ Scribed by Grove-Palmer, Fred
No coin nor oath required. For personal study only.
in nn oxygen-frcc ntmosplicrc, sacli as carbon diosiilc or nitrogen, bcforc mnking tlic ilctcrniiniitioii. 'J'liis is not easily cnrricd out in n works Inboriitory, so thc followin:: siniplc iinncnling process 1i:is bccii clcvisctl.
JIis 5 g. of tlic drillings wit11 0.5 p. of dry p o w l ~r r d crcillli of tiirtiir pliiccd in n porccliiin criiciblc of 1 2 in. diam. n t tlic top nnd I; iii. Iiigli, \vliicli is tlicn fillccl to tlic Lriiii with ii inistiire of 95% iicid-wrislicd .l~-inesli cnlcinctl sen-siind u i i d 5y(J po\vtlcrcd crciini of tiirtiir.
Plncc on it n silicii ciil~sule 11 in. intorniil tliririi. iilitl & in. tlccp. J n w r t iiiid fill in the spiicc on tlic outside bctwecn tlic crticil~lc niid tlic! cnpsuIlo wit11 tlir siiiidtiirtnr mixture 11s stio\vii in tlic skrtcli.
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