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Laboratory installation for the isolation of 2,2,6,6-tetrachlorocyclohexanone

✍ Scribed by Yu. I. Laz'yan; A. I. Bokanov; V. A. Kuzovkin; N. M. Dorofeeva; T. Yu. Talantova; V. G. Granik

Book ID
112713634
Publisher
Springer
Year
1994
Tongue
English
Weight
299 KB
Volume
28
Category
Article
ISSN
0091-150X

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## Abstract 6,6,6‐^2^H~3~‐2E‐Hexenal, leaf‐aldehyde, has been synthesized in 45% yield and 99.3% purity by reaction of 3,3,3‐^2^H~3~‐__n__‐propyl magnesium bromide with an ethereal solution of 3‐trimethylsiloxy‐2‐propenal (3) prepared __in situ__. This new one pot procedure alleviates the need to i