l,3,6,8-Tetra-tert-butyl-9-carbazyl:A Crystalline Monomeric Aminyl Radical

✍ Scribed by Doz. Dr. Franz A. Neugebauer; Hans Fischer

• Book ID: 101549169
• Publisher: John Wiley and Sons
• Year: 1971
• Tongue: English
• Weight: 209 KB
• Volume: 10
• Category: Article
• ISSN: 0044-8249
• DOI: 10.1002/anie.197107321

✦ Synopsis

sec-butyl acetate [(1-chloromethyI-2,3-dichloropropyl) acetate] ( I ) and 39% of the trichloro-n-butyl acetate [2,3,4trichlorobutyl acetate] (2) which are both composed of two diastereomers.

The other distillation fractions were not studied. A white solid crystallized from the high-boiling constituents (m. p.