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Kurzmitteilung / Short Communication A Convenient Preparation of Acetone Solutions of Dimethyldioxirane

✍ Scribed by Adam, Waldemar ;Bialas, Joachim ;Hadjiarapoglou, Lazaros

Book ID
101818388
Publisher
Wiley (John Wiley & Sons)
Year
1991
Tongue
English
Weight
122 KB
Volume
124
Category
Article
ISSN
0009-2940

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✦ Synopsis

Abstract

A novel simplified procedure affords consistently 0.09‐0.10 M solutions of distilled dimethyldioxirane in acetone; other than control of the reaction temperature below 15Β° and vigorous mechanical stirring, no other precautions are maniatory.

πŸ“œ SIMILAR VOLUMES

Oxidation of ketene-S,S-acetals, thioace
Oxidation of ketene-S,S-acetals, thioacetals, and thioketals by dimethyldioxirane: A convenient method for the preparation of bis-sulfones
✍ Denise Curi; Vera L. Pardini; Hans Viertler; Alfons L. Baumstark; Donald B. Hard πŸ“‚ Article πŸ“… 1994 πŸ› John Wiley and Sons 🌐 English βš– 549 KB

## Abstract The oxidation of a series of ketene‐S,S‐acetals, __2a__–__f__, and a series of thioacetals and thioketals, __4a__–__g__, with a fourfold or greater excess of dimethyldioxirane, __1__, produced the corresponding bis‐sulfones __3a__–__f__ and __5a__–__g__ in excellent yields. The reaction