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Kristallstruktur von [ZnH(NPMe3)]4, einem tetrameren Phosphaniminato-Komplex des Zinks mit terminalen Hydrido-Liganden

✍ Scribed by Matthias Krieger; Bernhard Neumüller; Kurt Dehnicke


Publisher
John Wiley and Sons
Year
1998
Tongue
German
Weight
51 KB
Volume
624
Category
Article
ISSN
0372-7874

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✦ Synopsis


The crystal structure of the title compound, which crystallizes as [ZnH(NPMe 3 )] 4 ´4 THF forming colourless, very reactive blocks, obtained by recrystallization from toluene, reveals discrete tetrameric molecules with heterocubane structure with almost undistorted Zn 4 N 4 cubic skeletons. The hydrido ligands assume terminal exocyclic positions with Zn±H bond lengths of 150 pm in average.