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Kishner Reduction of 3,3-Dimethyl-6-trifluoromethyl-1,2,3,4-tetrahydroindolo [2,3-c]quinolin-1-one.

✍ Scribed by A. V. Kibal'ny; A. A. Afonin


Publisher
John Wiley and Sons
Year
2005
Weight
13 KB
Volume
36
Category
Article
ISSN
0931-7597

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## Novel Conversion of Perfluoro(2,6-dimethyl-1-azacyclohexene) to 3,3,4,4,5-Pentafluoro-2,6-diphenyl-2,6-bis (trifluoromethyl)-1azabicyclo[3.1.0]hexane. -Treatment of perfluoro-azacyclohexene (I) with 2 equiv. of phenyllithium (V) in a cyclohexane/Et 2 O mixture provides access to azabicyclohex