A simple, sensitive, and selective method for rapid determination of nitrite is described which is based on its catalytic effect in the reaction between thymol blue and bromate in acidic media. The reaction is monitored spectrophotometrically by measuring the decrease in absorbance at 543 nm by a fi
Kinetic Spectrophotometric Determination of Traces of Sulfite Based on Its Additional Reaction with Methyl Green
โ Scribed by A. Jabbari; M. Shamsipur
- Publisher
- Elsevier Science
- Year
- 1993
- Tongue
- English
- Weight
- 252 KB
- Volume
- 48
- Category
- Article
- ISSN
- 0026-265X
No coin nor oath required. For personal study only.
โฆ Synopsis
A simple, rapid, and sensitive kinetic method has been developed for the determination of traces of sulfite ((0.05-2.5 \mu \mathrm{g} / \mathrm{ml})) based on the addition reaction of sulfite with methyl green at (\mathrm{pH} 8) and (25^{\circ} \mathrm{C}). The reaction is monitored spectrophotometrically by measuring the decrease in absorbance of the dyestuff at (625 \mathrm{~nm}) by the fixed time method. The limit of detection is (0.05 \mu \mathrm{g} / \mathrm{ml}) and the relative standard deviation for (0.5 \mu \mathrm{g} / \mathrm{ml}) sulfite is (2.88 %). The interfering effect of various ions was studied. The method was applied to the determination of sulfite in a number of fruit juices. 1993 Academic Press, Inc.
๐ SIMILAR VOLUMES
A sensitive kinetic fluorimetric flow injection method has been developed for the determination of Ag(I) over the range 100-2500 ng. The method is based on the catalytic effect of Ag(I) on the reduction reaction of safranine by iodide. Method development includes optimization of reagent concentratio