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Kinetic Resolution of Atropisomeric Amides

✍ Scribed by Rios, Ramon; Jimeno, Ciril; Carroll, Patrick J.; Walsh, Patrick J.

Book ID
127045377
Publisher
American Chemical Society
Year
2002
Tongue
English
Weight
57 KB
Volume
124
Category
Article
ISSN
0002-7863

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Kinetic resolution of sec-alcohols was performed by using axially chiral twisted amides, 4-(S)-alkyl 3-pivaloyl-l,3-thiazolidine-2-thiones (lb-ld and 2). The (S)-pivalates were selectively produced under neutral conditions; in contrast, the (R)-isomers were produced as major products in the presence