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Kinetic and thermodynamic control in the synthesis of methylglyoxal thioacetals from 2-ethoxypropenal

✍ Scribed by Nataliya A. Keiko; Evgeniya A. Funtikova; Lyudmila G. Stepanova; Yurii A. Chuvashev; Lyudmila I. Larina; Mikhail G. Voronkov

Book ID
119767898
Publisher
Royal Society of Chemistry
Year
2001
Tongue
English
Weight
88 KB
Volume
11
Category
Article
ISSN
0959-9436

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ChemInform Abstract: Kinetic and Thermod
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Stereoelectronic Effects and Chiral Recognition, II. Kinetic and Thermodynamic Control in the Formation of Chiral Thioacetals and Chiral Thioethers
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## Abstract The ratio of diastereomers obtained from chiral thiols 2 was shown to be time‐dependent both in thioacetal formation with lactol 1 (diastereomers 3/4) and in 1,4‐addition to nitrostyrene 5 (diastereomers 6/7, 8/9). An interpretation based on stereoelectronic effects is presented to expl