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Ketene dithio acetals as synthetic intermediates. Synthesis of unsaturated 1,5-diketones

✍ Scribed by Potts, Kevin T.; Cipullo, Michael; Ralli, Philip; Theodoridis, George


Book ID
118002821
Publisher
American Chemical Society
Year
1981
Tongue
English
Weight
301 KB
Volume
103
Category
Article
ISSN
0002-7863

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4, ## Experimental Part 1. General. Solvents were either reagent or technical grade and when necessary were purified and dried by distillation from an appropriate dessiccant under N,. S o h . after reactions and extractions were evaporated at ca. 20 Torr. HMPA = hexamethylphosphoric triamide. M.p