K2AlF5 · H2O: Location of hydrogen atoms by X-ray diffraction and Raman spectroscopy study
✍ Scribed by J.L. Fourquet; B. Boulard; F. Plet
- Publisher
- Elsevier Science
- Year
- 1989
- Tongue
- English
- Weight
- 317 KB
- Volume
- 81
- Category
- Article
- ISSN
- 0022-4596
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The crystal structure of La(H 2 O) 2 K(C 2 O 4 ) 2 ' H 2 O has been solved ab initio from powder di4raction data collected with conventional monochromatic X-rays. The symmetry is monoclinic, space group C2/m, cell dimensions a ؍ 22.033(1) A > , b ؍ 7.6003(5) A > , c ؍ 6.6418(4) A > , ؍ 103.8
The structure of Ag 2 Ce(H 2 O)(NO 3 ) 5 was determined from single-crystal diffraction. The symmetry is monoclinic (space group P2/c): a ؍ 21.472(5), b ؍ 8.027(1), c ؍ 15.413(3) A s , ؍ 90.45(2)°, V ؍ 2656.2(7) A s , Z ؍ 8. The structure consists of infinite chains of Ce icosahedra link