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J -GFT NMR for Precise Measurement of Mutually Correlated Nuclear Spin−Spin Couplings

✍ Scribed by Atreya, Hanudatta S.; Garcia, Erwin; Shen, Yang; Szyperski, Thomas

Book ID
126910220
Publisher
American Chemical Society
Year
2007
Tongue
English
Weight
599 KB
Volume
129
Category
Article
ISSN
0002-7863

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We describe a method for measuring nuclear magnetic dipole-dipole couplings in NMR spectra of solids undergoing rapid magic angle spinning (MA?+). We show in theory, simulations, and experiments that the couplings, which are averaged out by MAS alone, can be recovered by applying simple resonant rad