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Isolation of spatulenol and (−)-caryophyllene oxide from Vernonia mollissima don and 1H and 13C reassignment by two-dimensional NMR spectroscopy

✍ Scribed by H. C. Krebs; J. V. Rakotoarimanga; G. G. Habermehl


Publisher
John Wiley and Sons
Year
1990
Tongue
English
Weight
219 KB
Volume
28
Category
Article
ISSN
0749-1581

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✦ Synopsis


Abstract

Two sesquiterpenoids, spatulenol and (−)‐caryophyllene oxide, were isolated from the hexane extract of the Brazilian plant Vernonia mollissima Don. The ^1^H and ^13^C NMR spectra of these compounds have been reassigned completely by COSY experiments and ^13^C/^1^H shift correlation diagrams.


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