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Isolation of Acyl Thioacyl Sulfides

✍ Scribed by Prof. Dr. Shinzi Kato; Katsumi Sugino; Masatoshi Yamada; Tomonori Katada; Prof. Dr. Masateru Mizuta

Publisher: John Wiley and Sons
Year: 1977
Tongue: English
Weight: 192 KB
Volume: 16
Category: Article
ISSN: 0044-8249
DOI: 10.1002/anie.197708791

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## Abstract A number of unsymmetrical acyl thioacyl sulfides [RC(S)S(O)CR'] have been prepared and characterized by the reaction of piperidinium or sodium dithiocarboxylates with acyl chlorides or by desulfurization reaction of acyl thioacyl disulfides with triphenylphosphine. They are deep blue oi

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## Abstract Reaction of dithioic acids with dicyclohexylcarbodiimide has been found to give the corresponding bis(thioacyl) sulfides **1** in good yield, which are very useful thioacylating reagents under mild reaction conditions. Most of the aromatic thioanhydrides (**1**, R = aromatic) are fairly