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Isolation, Characterization and Structure of α-Lipoic Acid 1

✍ Scribed by Reed, Lester J.; Gunsalus, I. C.; Schnakenberg, G. H. F.; Soper, Quentin F.; Boaz, Harold E.; Kern, Stanley F.; Parke, Thomas V.


Book ID
121195551
Publisher
American Chemical Society
Year
1953
Tongue
English
Weight
496 KB
Volume
75
Category
Article
ISSN
0002-7863

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NMR Spectroscopic Characterization of Is
✍ Arndt Müller; Martin Knaack; Alfred Olbrich 📂 Article 📅 1997 🏛 John Wiley and Sons 🌐 English ⚖ 215 KB 👁 1 views

a-Lipoic acid (thioctic acid) was oxidized in saturated solution by means of hydrogen peroxide. The NaHCO 3 resulting mixture of four structurally isomeric S-oxides (b-lipoic acids, thiosulÐnates) was characterized by NMR spectroscopy without chromatographic separation. The regio-and stereochemistry