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Isolation and Proof of Structure of 1,1,4,4-Tetramethyl-6-t-butyl-1,2,3,4- tetrahydronaphthalene 1

✍ Scribed by MYHRE, PHILIP C.; SCHUBERT, W. M.

Book ID: 120388830
Publisher: American Chemical Society
Year: 1960
Tongue: English
Weight: 523 KB
Volume: 25
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo01075a008

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study ( < -30"C)1111. This is best evidenced by the upfield shift of protons H' (by 23Hz) and H5 (by 32Hz) on going from ( 3 ) to ( 5 ) , which simply reflects the increased availability of the lone pair for limited delocalization but is clearly inconsistent with the development of the diamagnetic r