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Isolation and determination of carbendazim residue from wheat grain by matrix solid-phase dispersion and HPLC

✍ Scribed by Monika Michel; Bogusław Buszewski

Publisher
John Wiley and Sons
Year
2003
Tongue
English
Weight
365 KB
Volume
26
Category
Article
ISSN
1615-9306

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✦ Synopsis

Abstract

Carbendazim residues were analyzed by column‐switching high‐performance liquid chromatography (HPLC) with photodiode array detection (PDA). The active ingredient was extracted by matrix solid‐phase dispersion (MSPD) from wheat grain on an acidic silica gel column using a methanol‐dichloromethane mixture. The recovery rate for fortified samples was 87.3 ± 3.3% with a standard deviation (SD) of 2.9%. The detection limit was 0.02 μg/mL. The method was applied to the determination of carbendazim residues in wheat grain samples from a treated field.

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