The use of temperatures higher than 30°0 during the hydration of 1:3 high alumina cement mortar leads to the formation of the cubic hydra te C3AH~, hence avoiding the conversion of CAHIo to C3AH 6. The subsequent-carbonation of 03AH 6 with 002 and therm~l treatm@nt leads to the formation of stable c
✦ LIBER ✦
IR studies of PAN fibres thermally stabilized at elevated temperatures
✍ Scribed by J. Mittal; O.P. Bahl; R.B. Mathur; N.K. Sandle
- Publisher
- Elsevier Science
- Year
- 1994
- Tongue
- English
- Weight
- 317 KB
- Volume
- 32
- Category
- Article
- ISSN
- 0008-6223
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✦ Synopsis
It
was proposed earlier that the additional exothermic peak observed at 350°C in differential scanning calorimetry of PAN fibre is associated with certain intermolecular cross linking, as well as to the aromatization of structure, which results in a better stabilized structure. It has been further confirmed in the present study through infrared spectroscopy that these reactions take place in the fibre and occur only in the presence of oxygen.
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