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Ionic Liquid Modification of Layered Silicates for Enhanced Thermal Stability

✍ Scribed by Cormac Byrne; Tony McNally


Publisher
John Wiley and Sons
Year
2007
Tongue
English
Weight
157 KB
Volume
28
Category
Article
ISSN
1022-1336

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✦ Synopsis


Abstract

A natural and synthetic layered silicate (LS) was modified with trihexyltetradecyl‐phosphonium tetrafluoroborate (an ionic liquid) via a cationic exchange reacation. The exchange reaction and loading of modifier was investigated using a combination of WAXD, inductively coupled plasma‐optical emmission spectroscopy (ICP‐OES) and thermogravimetric analysis (TGA). The thermal stability of the modified LS was enhanced by up to 150 °C, when compared with conventional quaternary ammonium cations, making melt mixing of such modified nanoclays possible with poly(ethylene‐terephthalate) (PET).

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