## Abstract Boehmite [AlOOH] nanoneedles, nanorods, and nanotubes were successfully synthesized by a facile sol‐hydrothermal method without using any surfactant. Calcination of the corresponding boehmite nanostructures at 700 °C gave the corresponding γ‐Al~2~O~3~ nanoneedles, nanorods, and nanotube
Ionic liquid-assisted hydrothermal synthesis of γ-Al2O3hierarchical nanostructures
✍ Scribed by Tongil Kim; Haobo Li; Jiabiao Lian; Huaihai Jin; Jianmin Ma; Xiaochuan Duan; Gang Yao; Wenjun Zheng
- Publisher
- John Wiley and Sons
- Year
- 2010
- Tongue
- English
- Weight
- 191 KB
- Volume
- 45
- Category
- Article
- ISSN
- 0232-1300
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✦ Synopsis
The boehmite (Al 2 O 3 •H 2 O) hierarchical nanostructure with spindle-like morphology has been successfully synthesized via ionic liquid-assisted hydrothermal synthetic method under mild condition using an ionic liquid 1-butyl-3-dimethylimidazolium bromide ([Bmim][Br]) as a template. The proposed formation mechanism has been investigated and the hydrogen bond-co-π-π stack mechanism is used to be responsible for the present formation of the precursor hierarchical nanostructure. The γ-Al 2 O 3 hierarchical nanostructure was obtained by calcining the as-synthesized precursor at 500 °C for 2 h, preserving the same morphology.
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