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Iodo­triphenyl­tin(IV): a monoclinic polymorph

✍ Scribed by Mao, Wu-Tao ;Tian, Lai-Jin ;Gu, Ke-Qiang ;Sun, Yu-Xi

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
149 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

A monoclinic polymorph of the title compound, [Sn(C 6 H 5 ) 3 I], complements the previously reported triclinic variant [Ng (1995). Acta Cryst. C51, 629-631;Simard & Wharf (1994). Acta Cryst. C50, 397-403]. There are two molecules in the asymmetric unit; in both cases, the Sn atom adopts a distorted SnIC 3 tetrahedral environment.

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Single-crystal X-ray study T = 293 K Mean (C-C) = 0.005 A R factor = 0.035 wR factor = 0.097 Data-to-parameter ratio = 15.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.