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Iodobenzene diacetate on alumina: Efficient synthesis of 1,3,4-oxadiazolyl-1,8-naphthyridines in solventless system using microwaves

✍ Scribed by K. Mogilaiah; J. Uma Rani; B. Sakram; N. Vasudeva Reddy

Book ID: 102345886
Publisher: Journal of Heterocyclic Chemistry
Year: 2006
Tongue: English
Weight: 215 KB
Volume: 43
Category: Article
ISSN: 0022-152X
DOI: 10.1002/jhet.5570430235

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✦ Synopsis

oxadiazol-2-ylmethyl)-3-(p-methoxyphenyl)-1H-[1,8]naphthyridin-2-ones (5) were synthesized by the oxidative cyclization of [2-oxo-3-(p-methoxyphenyl)-2H-[1,8]naphthyridin-1-yl]acetic acid arylidene-hydrazides (4) with alumina-supported iodobenzene diacetate (IBD) in solvent-free conditions under microwave irradiation. The products are obtained in good yields and in a state of high purity.

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