✦ LIBER ✦
Iodinated Biaryls Synthesized by the Direct Dehydrodimerization of Iodoarenes Using Phenyliodine(III) Bis(trifluoroacetate) (PIFA)
✍ Scribed by Daniela Mirk; Alexander Willner; Roland Fröhlich; Siegfried R. Waldvogel
- Publisher
- John Wiley and Sons
- Year
- 2004
- Tongue
- English
- Weight
- 130 KB
- Volume
- 346
- Category
- Article
- ISSN
- 1615-4150
No coin nor oath required. For personal study only.
✦ Synopsis
Abstract
Multiply iodinated biaryls can be prepared in yields up to 75% by direct oxidative coupling reaction of the iodinated arenes. The PIFA‐mediated dehydrodimerization is superior to all other known methods. The developed protocol is reliable and easy to perform.