The structure of blends of Nylon 6 with deuterated polyaniline emeraldine base (D-PANI-EB) and fully doped D-PANI salts (D-PANI-ES) formed from camphorsulfonic acid (CSA), methanesulfonic acid (MSA), or dodecyl benzenesulfonic acid (DBSA) were investigated by small-angle neutron (SANS) and X-ray sca
Investigation of metal foam formation by microscopy and ultra small-angle neutron scattering
β Scribed by J. Banhart; D. Bellmann; H. Clemens
- Publisher
- Elsevier Science
- Year
- 2001
- Tongue
- English
- Weight
- 386 KB
- Volume
- 49
- Category
- Article
- ISSN
- 1359-6454
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β¦ Synopsis
Zinc foams were prepared by applying the powder compaction method which comprises mixing zinc powder with a small fraction of a blowing agent, compacting this mix and creating a foam by heat treatment above the melting temperature of the metal. The foaming process which normally leads to a volume expansion of some 500% was artificially stopped in very early stages by quenching. The resulting samples with porosities below 20% were then characterised by microscopy and ultra small-angle neutron scattering (USANS). Foam microstructures, pore morphologies, the locations of the blowing agent particles, pore and particle size distributions and total pore volume fractions were determined. Two mechanisms for pore formation could be identified by microscopy. The pore growth behaviour for different size regimes could be obtained from the USANS distribution curves, thus giving insight into the early stages of metal foam formation.
π SIMILAR VOLUMES
The ultra-small-angle X-ray and neutron scattering techniques are useful techniques for the investigation of colloidal systems. The very high small-angle resolution of these scattering techniques has provided important and novel information to elucidate the formation mechanism of colloidal crystals.