Thermal Analysis is a well-established set of techniques for obtaining qualitative and quantitative information about the effects of various heat treatments on materials of all kinds, including new chemical compounds, plastics, ceramics, alloys, construction materials, minerals, foods and medicines.
Introduction to Thermal Analysis: Techniques and applications
โ Scribed by Michael E. Brown (auth.)
- Publisher
- Springer Netherlands
- Year
- 1988
- Tongue
- English
- Leaves
- 219
- Edition
- 1
- Category
- Library
No coin nor oath required. For personal study only.
โฆ Synopsis
The aim of this book is, as its title suggests, to help sOilleone with little or no knowledge of what thermal analysis can do, to find out briefly what the subject is all about, to decide whether it will be of use to him or her, and to help in getting started on the more common techniques. Some of the less-common techniques are mentioned, but more specialized texts should be consulted before venturing into these areas. This book arose out of a set of notes prepared for courses on thermal analysis given at instrument workshops organized by'the S.A. Chemical Institute. It has also been useful for similar short courses given at various universities and technikons. I have made extensive use ofthe manufacturers' literature, and I am grateful to them for this information. A wide variety of applications has been drawn from the literature to use as examples and these are acknowledged in the text. A fuller list of the books, reviews and other literature ofthermal analysis is given towards the back of this book. The ICTA booklet 'For Better Thermal Analysis' is also a valuable source of information. I am particularly grateful to my wife, Cindy, for typing the manuscript, to Mrs Heather Wilson for the line drawings, and to Professor David Dollimore of the University of Toledo, Ohio, for many helpful suggestions.
โฆ Table of Contents
Front Matter....Pages i-x
Introduction....Pages 1-4
Thermal events....Pages 5-6
Thermogravimetry (TG)....Pages 7-22
Differential thermal analysis (DTA) and differential scanning calorimetry (DSC)....Pages 23-49
Thermoptometry....Pages 50-55
Thermodilatometry (TD)....Pages 56-62
Thermomechanical analysis (TMA)....Pages 63-68
Dynamic mechanical analysis (DMA) or dynamic thermomechanometry....Pages 69-80
Combination of thermal analysis techniques....Pages 81-85
Evolved gas analysis (EGA)....Pages 86-98
Less-common techniques....Pages 99-116
The use of microcomputers in thermal analysis....Pages 117-126
Reaction kinetics from thermal analysis....Pages 127-151
Purity determination using DSC....Pages 152-162
The literature and nomenclature of thermal analysis....Pages 163-167
Thermal analysis equipment....Pages 168-169
Conclusion....Pages 170-170
Back Matter....Pages 171-211
โฆ Subjects
Polymer Sciences; Physical Chemistry; Inorganic Chemistry
๐ SIMILAR VOLUMES
<p>to Thermal Analysis Techniques and Applications Edited by Michael E. Brown Chemistry Department, Rhodes University, Grahamstown, South Africa KLUWER ACADEMIC PUBLISHERS NEW YORK, BOSTON, DORDRECHT, LONDON, MOSCOW eBook ISBN: 0-306-48404-8 Print ISBN: 1-4020-0472-9 ยฉ2004 Kluwer Academic Publishers
Thermal Analysis is a well-established set of techniques for obtaining qualitative and quantitative information about the effects of various heat treatments on materials of all kinds, including new chemical compounds, plastics, ceramics, alloys, construction materials, minerals, foods and medicines.
<span>to Thermal Analysis Techniques and Applications Edited by Michael E. Brown Chemistry Department, Rhodes University, Grahamstown, South Africa KLUWER ACADEMIC PUBLISHERS NEW YORK, BOSTON, DORDRECHT, LONDON, MOSCOW eBook ISBN: 0-306-48404-8 Print ISBN: 1-4020-0472-9 ยฉ2004 Kluwer Academic Publish
Dynamic mechanical analysis has left the exclusive domain of the rheologist, becoming a prevalent tool in the analytical laboratory. This practical introduction to the field provides a starting point from which to delve into the applications of DMA, its workings, and its advantages and limitations.