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Interpretation of proton chemical shift tensors

✍ Scribed by K.F. Lau; R.W. Vaughan

Book ID
111708435
Publisher
Elsevier Science
Year
1975
Tongue
English
Weight
532 KB
Volume
33
Category
Article
ISSN
0009-2614

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Proton nuclear magnctlc shxldmg tensors arc calculated for some O-H...0 hydrogen bonds. (H302); (HzO)z, and (H50~)+. The effects of charge, geometry. and bws set are stuled. Agreement ~7th single crystal p&cd NhlR evperimcnts is obtamcd. A Itneer dependence betwcn the proton chcmwal shift and the 0.

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The proton chemical shift tensor of the hgdroxyl proton in calci;m hydroxide has been measured using multiple pulse NMR techkques. The tensor is axially symmetric with susceptibility corrected components 01= -9.3 \* 1 ppm and 01 = +4.7 i 1 ppm relative to TM%