Interlaboratory Study to Improve the Quality Control of Methylmercury Determination in Sediment

✍ Scribed by Ph. Quevauviller; G. U. Fortunati; M. Filippelli; F. Baldi; M. Bianchi; H. Muntau

• Publisher: John Wiley and Sons
• Year: 1996
• Tongue: English
• Weight: 638 KB
• Volume: 10
• Category: Article
• ISSN: 0268-2605
• DOI: 10.1002/(sici)1099-0739(199609)10:7<537::aid-aoc507>3.0.co;2-n

✦ Synopsis

The results are presented of an interlaboratory study on methylmercury (MeHg) in sediment carried out by a group of European laboratories within the framework of a project managed by the EC Standards, Measurements and Testing Programme (formerly BCR). The aim of this exercise was to evaluate the performance of current methods used for MeHg determination in sediment in order to improve the state-of-the-art prior to the certification of a candidate reference material. The paper describes the organization of the interlaboratory study, the preparation of the sediment material used, the techniques evaluated and the results obtained by the participating laboratories. The outcome of the collaborative project showed that certification could be contemplated, providing that certain analytical techniques were optimized, especially with regard to extraction methods.