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Interference by hydrogen peroxide in the assay for tryptophan with p-dimethylaminobenzaldehyde by the method of spies and chambers

✍ Scribed by Bibhuti R. DasGupta

Publisher
Elsevier Science
Year
1969
Tongue
English
Weight
216 KB
Volume
30
Category
Article
ISSN
0003-2697

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## Abstract It was found that __tert__‐BuNH~2~ is an efficient catalyst for epoxidation of __Ξ±__,__Ξ²__‐unsaturated ketones with 30% H~2~O~2~ under mild conditions. For most of the cyclic unsaturated ketones used, moderate to excellent yields (45%–93%) were obtained within 24 h period.