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Intercalation of Platinum Complex in LDH Compounds

✍ Scribed by P. Beaudot; M.E. De Roy; J.P. Besse

Publisher: Elsevier Science
Year: 2001
Tongue: English
Weight: 466 KB
Volume: 161
Category: Article
ISSN: 0022-4596
DOI: 10.1006/jssc.2001.9322

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✦ Synopsis

Intercalation of platinum complex was carried out in [ZnAl],

[MgAl], and [CuAl] LDH matrix by a new method including hydrothermal synthesis. Free carbonate products were obtained. XRD and FTIR studies show the total exchange. However, the geometry of the local environment of the platinum atom in the complex appeared to be modi5ed during intercalation. By thermal treatments and reduction in ethylene glycol, metallic particles dispersed on oxide powder were obtained. The resulting calcined products could have some interest in heterogeneous catalysis.

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