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Interaction of Sulfonated Calix[n]arenes with Rhodamine B and Its Application to Determine Acetylcholine in a Real Neutral Aqueous Medium

✍ Scribed by Yong-Jun Zhang; Wei-Xiao Cao; Jian Xu


Publisher
John Wiley and Sons
Year
2010
Tongue
English
Weight
284 KB
Volume
20
Category
Article
ISSN
0256-7660

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✦ Synopsis


Abstract

Complexation between Rhodamine B (RB) and sulfonated calix [n] arenes (SC__n__A) were studied by means of UV‐vis spectroscopy and fluorescence spectroscopy. In the presence of sulfonated calix[n] arenes, the absorption band of Rhodamine B shifts to longer wavelength and its intensity decreases. The formation of a host‐guest type complex also results in the fluorescence quenching of Rhodamine B. The association constants for the RB/SC__n__A complexes increase in the order of SC4A < SC6A < SC8A and show dependence on the size of the cavities of the calixarenes. The fluorescence is selectively regenerated by adding acetylcholine. Based on this observation, a method to determine acetylcholine in a real neutral aqueous medium was developed.