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Interaction of Methimazole with I 2 : X-ray Crystal Structure of the Charge Transfer Complex Methimazole−I 2 . Implications for the Mechanism of Action of Methimazole-Based Antithyroid Drugs

✍ Scribed by Isaia, Francesco; Aragoni, M. Carla; Arca, Massimiliano; Demartin, Francesco; Devillanova, Francesco A.; Floris, Giovanni; Garau, Alessandra; Hursthouse, Michael B.; Lippolis, Vito; Medda, Rosaria; Oppo, Fabio; Pira, Marilena; Verani, Gaetano

Book ID
120345629
Publisher
American Chemical Society
Year
2008
Tongue
English
Weight
99 KB
Volume
51
Category
Article
ISSN
0022-2623

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## Abstract The reaction of 2‐mercaptopyridine (C~5~H~5~NS or PYSH) with diiodine in a molar ratio of 1:2 in dichloromethane led to the oxidation and dimerization of the ligand and formation of [(PYS−PYSH)^+^·I~3~^−^]. The compound was characterised by elemental analysis, DTA‐TG, FT‐Raman, FT‐IR, U