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Interaction of dimethyltin sulfide with 1,2-dibromoethane. Crystal structure of the dimethyltin dibromide /1,4-dithiane complex.

✍ Scribed by V.I. Shcherbakov; I.K. Grigor'eva; G.A. Razuvaev; L.N. Zakharov; R.I. Bochkova; Yu.T. Struchkov

Publisher: Elsevier Science
Year: 1987
Tongue: English
Weight: 541 KB
Volume: 319
Category: Article
ISSN: 0022-328X
DOI: 10.1016/0022-328x(87)80345-5

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## Abstract The reactions of diorganotin dichloride [Ph~2~SnCl~2~, (PhCH~2~)~2~‐SnCl~2~ or (__n__‐Bu)~2~SnCl~2~] with potassium salt of 2, 5‐dimercapto‐4‐phenyl‐1, 3, 4‐thiodiazole gave complexes R~2~Sn (S~3~N~2~C~8~H~5~)~2~ (4: R = Ph; 5: R = PhCH~2~ and 6: R = __n__‐Bu), respectively. Characteriz