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‘Intelligent’ fraction collection to improve structural characterization by mass spectrometry

✍ Scribed by Dieter M. Drexler; Philip R. Tiller


Publisher
John Wiley and Sons
Year
1998
Tongue
English
Weight
267 KB
Volume
12
Category
Article
ISSN
0951-4198

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✦ Synopsis


A method to collect high performance liquid chromatography (HPLC) fractions in an automated manner based upon mass spectrometric data is described. The use of modern ion-trap mass spectrometry affords molecular mass, structural data and the collection of fractions of interest for further analyses throughout the course of a single HPLC/MS experiment. This eliminates the need for additional HPLC/MS analyses to obtain further structural information. An example of such a multiplexed experiment is given.