## Abstract A variable‐temperature ^1^H‐NMR study and X‐ray structural analysis show that the most stable conformational isomer of [3.3](2,6)pyridinophane 2 is the __syn__(boat‐boat) conformer, and the relative stability order of the three stable conformers is __syn__(boat‐boat) > __syn__(chair‐boa
✦ LIBER ✦
Insight Into the Conformational Arrangement of a Bis-THF Diol Compound Through 2D-NMR Studies and X-Ray Structural Analysis
✍ Scribed by Vincenzo Piccialli; Sabrina Zaccaria; Roberto Centore; Angela Tuzi; Nicola Borbone; Giorgia Oliviero; Stefano D’Errico; Valentina D’Atri
- Book ID
- 113070403
- Publisher
- Springer
- Year
- 2011
- Tongue
- English
- Weight
- 415 KB
- Volume
- 42
- Category
- Article
- ISSN
- 1572-8854
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Proton-proton cross-relaxation rates have been measured for the trisaccharide beta-D-Glcp-(l --> 2)[beta-D-Glcp-(1 --> 3)]alpha-D-Glcp-OMe in D2O as well as in D2O/[D6]DMSO 7:3 solution at 30 degrees C by means of one-dimensional NMR pulsed field gradient 1H,1H NOESY and TROESY experiments. Interato